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Quality assessment and control measures are in place to ensure that the measurement process is stable and under control [2, 8] Within QC, internal and external quality control are distinguished In general, QA comprises the following topics as also schematized in Figure 6 Use of Validated Methods: In-House Versus Interlaboratory Validation Wherever possible or practically achievable, a laboratory should use methods which have been fully validated through a collaborative trial, also called interlaboratory study or method performance study Validation in collaborative studies is required for any new analytical method before it can be published as a standard method (see below) However, single-laboratory validation is a valuable source of data usable to demonstrate the tness for purpose of an analytical method In-house validation is of particular interest in cases where it is inconvenient or impossible for a laboratory to enter into or to organize itself a collaborative study [4, 5].
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Any project begins with requirements gathering. If you don t have a good understanding of the customers needs, you have little chance of building an effective solution for the customers problems. This chapter described the requirements gathering phase for The Pampered Pet database project. In this chapter, you saw examples of: Meeting with customers to identify requirements. Building a mockup to increase customer understanding, buy-in, and enthusiasm. De ning the database s main entities and their relationships. Determining data integrity requirements for entities. De ning and writing use cases.
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which we wish to solve for t 0 given x(0), where x(t) = [x0 (t) x1 (t) xm 1 (t)]T . If we also de ne f (x(t), t) = [f0 (x(t), t) f1 (x(t), t) fm 1 (x(t), t)]T , then we may express (10.156) in compact vector form as dx(t) = f (x(t), t). dt (10.157)
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On the one hand, even if an in-house validated method shows good performance and reliable accuracy, such a method cannot be adopted as a standard method Inhouse validated methods need to be compared between at least eight laboratories in a collaborative trial On the other hand, a collaborative study should not be conducted with an unoptimized method [58] Interlaboratory studies are restricted to precision and trueness while other important performance characteristics such as speci city and LOD are not addressed [105] For these reasons, single-laboratory validation and interlaboratory validation studies do not exclude each other but must be seen as two necessary and complementary stages in a process, presented in Figure 9 The added value of single-laboratory validation is that it simpli es the next step interlaboratory validation and thereby minimizes the gap between internally (validated or not) developed methods and the status of interlaboratory validation.
3G mobile wireless technology is based on direct sequence code division multiple access (DS-CDMA). The signal bandwidth is 5 MHz, which is larger that the coherence bandwidth of the transmission channels. Consequently, the signal is subject to wideband propagation, i.e., frequency selective fading is observed at the receiver. Thus the term wideband CDMA is used for the technology. Data rates of up to 384 kb/s have been predicted and location awareness of the users is a legal requirement for operation of any mobile telephone system in Europe and North America. The standard for 3G is referred to as Universal Mobile TelecommunicationsSystem or UMTS. This covers the complete system including the wireless section and core network. The wireless section of the standard is called UMTS Terrestrial Wireless Access or UTRA. Duplex transmissions are made using frequency division duplex (FDD) and the uplink and downlink channels are separated by around 120MHz. Transmit, or downlink beamforming, provides additional challenges to the system designer when operating an FDD system which have been described in chapter 5 . Switched beam antennas, which have been described in chapter 4, are an alternative to the fully adaptive, computational intensive downlink beamforming
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